ES9002 ENVIRONMENTAL QUALITY MONITORING SYLLABUS | ANNA UNIVERSITY ME/M.Tech ENVIRONMENTAL SCIENCE AND ENGINEERING ELECTIVE SYLLABUS REGULATION 2009 2011 2012-2013 BELOW IS THE ANNA UNIVERSITY ELECTIVE M.E/M.Tech ENVIRONMENTAL SCIENCE AND ENGINEERING DEPARTMENT SYLLABUS, TEXTBOOKS, REFERENCE BOOKS,EXAM PORTIONS,QUESTION BANK,PREVIOUS YEAR QUESTION PAPERS,MODEL QUESTION PAPERS, CLASS NOTES, IMPORTANT 2 MARKS, 8 MARKS, 16 MARKS TOPICS. IT IS APPLICABLE FOR ALL STUDENTS ADMITTED IN THE YEAR 2011 2012-2013 (ANNA UNIVERSITY CHENNAI,TRICHY,MADURAI,TIRUNELVELI,COIMBATORE), 2009 REGULATION OF ANNA UNIVERSITY CHENNAI AND STUDENTS ADMITTED IN ANNA UNIVERSITY CHENNAI DURING 2010
ES9002 ENVIRONMENTAL QUALITY MONITORING L T P C
3 0 0 3
OBJECTIVE:
To educate the students on the various instrumental methods of monitoring the quality
of air, water and soil.
UNIT I INTRODUCTION 9
Wet Chemistry methods and their limitations-Instrumental Methods, Selection of method-
Precision and Accuracy, Error in measuring signals- Quality control & assurance-
Sample preservation, Sample preparation and analyte isolation.
UNIT II SPECTROSCOPIC METHODS 12
Principles, techniques and applications of spectrophotometry, fluorimetry, nephelometry
and turbidimetry, Atomic Absorption Spectrometry (Flame, graphite furnace and hydride
generation), Atomic Emission Spectrometry (AES) , flame and Inducted Coupled
Plasma (ICP) – TOC Analyzer
UNIT III CHROMATROGRAPHIC METHODS 8
Column, Paper and thin layer chromatography (TLC)- Principles, techniques and
applications of GC, GC-MS, High performance liquid chromatography (HPLC) and Ion
chromatograph (IC)-Hyphenated techniques for Environmental contaminant(trace
organics) analysis.
UNIT IV ELECTRO AND RADIO ANALYTICAL METHODS 8
Principles, techniques and applications of Conductometry, potentiometry, coulometry,
AOX analyzer Amperometry, polarography, New Activation Analysis (NAA), X-ray
Fluorescence (XRF) and X-ray Diffraction (XRD) methods.
UNIT V CONTINUOUS MONITORING INSTRUMENTS 8
Principles, techniques and applications of NDIR analyzer for CO, chemiluminescent
analyzer for NOx Fluorescent analyzer for SO2- Particulates analysis- Auto analyzer for
water quality using flow injection analysis.
TOTAL: 45 PERIODS
11
REFERENCES:
1. Willard H. Merritt, L. Dean, D.A. and Settle, F.A. ‘Instrumental methods of
analysis Edn. Words Worth, New York, 2004.
2. Paul R. Loconto Trace Environmental Quantitative Analysis: Principles,
Techniques, and Applications, Marcel Dekker; 1 edition (May 2001),
3. Ewing Instrumental Methods of Chemical Analysis, 5th Edition, McGraw Hill, New
York.1985
4. Reeve, R.N., “Introduction to Environmental Analysis”, Analytical Techniques in
the Sciences, John Wiley & Sons, Chichester, UK, 2002.
5. Barceló, D.(editor), “Environmental analysis. Techniques, Applications and
Quality Assurance”, Elsevier, The Netherlands, 1996
ES9002 ENVIRONMENTAL QUALITY MONITORING L T P C
3 0 0 3
OBJECTIVE:
To educate the students on the various instrumental methods of monitoring the quality
of air, water and soil.
UNIT I INTRODUCTION 9
Wet Chemistry methods and their limitations-Instrumental Methods, Selection of method-
Precision and Accuracy, Error in measuring signals- Quality control & assurance-
Sample preservation, Sample preparation and analyte isolation.
UNIT II SPECTROSCOPIC METHODS 12
Principles, techniques and applications of spectrophotometry, fluorimetry, nephelometry
and turbidimetry, Atomic Absorption Spectrometry (Flame, graphite furnace and hydride
generation), Atomic Emission Spectrometry (AES) , flame and Inducted Coupled
Plasma (ICP) – TOC Analyzer
UNIT III CHROMATROGRAPHIC METHODS 8
Column, Paper and thin layer chromatography (TLC)- Principles, techniques and
applications of GC, GC-MS, High performance liquid chromatography (HPLC) and Ion
chromatograph (IC)-Hyphenated techniques for Environmental contaminant(trace
organics) analysis.
UNIT IV ELECTRO AND RADIO ANALYTICAL METHODS 8
Principles, techniques and applications of Conductometry, potentiometry, coulometry,
AOX analyzer Amperometry, polarography, New Activation Analysis (NAA), X-ray
Fluorescence (XRF) and X-ray Diffraction (XRD) methods.
UNIT V CONTINUOUS MONITORING INSTRUMENTS 8
Principles, techniques and applications of NDIR analyzer for CO, chemiluminescent
analyzer for NOx Fluorescent analyzer for SO2- Particulates analysis- Auto analyzer for
water quality using flow injection analysis.
TOTAL: 45 PERIODS
11
REFERENCES:
1. Willard H. Merritt, L. Dean, D.A. and Settle, F.A. ‘Instrumental methods of
analysis Edn. Words Worth, New York, 2004.
2. Paul R. Loconto Trace Environmental Quantitative Analysis: Principles,
Techniques, and Applications, Marcel Dekker; 1 edition (May 2001),
3. Ewing Instrumental Methods of Chemical Analysis, 5th Edition, McGraw Hill, New
York.1985
4. Reeve, R.N., “Introduction to Environmental Analysis”, Analytical Techniques in
the Sciences, John Wiley & Sons, Chichester, UK, 2002.
5. Barceló, D.(editor), “Environmental analysis. Techniques, Applications and
Quality Assurance”, Elsevier, The Netherlands, 1996
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